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Journal of Ceramic Science and Technology

The Journal of Ceramic Science and Technology publishes original scientific articles on all topics of ceramic science and technology from all ceramic branches. The focus is on the scientific exploration of  the relationships between processing, microstructure and properties of sintered ceramic materials as well as on new processing routes for innovative ceramic materials. The papers may have either theoretical or experimental background. A high quality of publications will be guaranteed by a thorough double blind peer review process.

The Journal is published by Göller Verlag GmbH on behalf of the Deutsche Keramische Gesellschaft (DKG). Edited by Yu-Ping Zeng, Shanghai Institute of Ceramics, Chinese Academy of Sciences, China.

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Investigation of Chemically Modified ICIE16 Bioactive Glass, Part II

F.J. Hmood1, F. Schmidt2, O. Goerke3, J. Günster2

1 University of Babylon, Al Hillah, Babylon, Iraq
2 BAM Bundesanstalt für Materialforschung und -prüfung, Unter den Eichen 87, D-12205 Berlin, Germany
3 Technische Universitat Berlin, Straße des 17. Juni 135, D-10623 Berlin, Germany

received April 24, 2019, received in revised form August 15, 2019, accepted October 24, 2019

Vol. 11, No. 1, Pages 1-10   DOI: 10.4416/JCST2019-00031

Abstract

Chemically modified bioactive glasses based on ICIE16 were prepared with the melt-quenching method using water as a quenching medium. The sinterability of these bioactive glasses was investigated and is discussed in this article. The sintering experiments were conducted with different sintering temperatures, sintering times and heating rates. Those parameters are crucial for dense glass with an amorphous structure. The particle size (d50) of the starting glass powder was determined at 88 µm and kept constant. The pre-pressed glass pellets were cold-isostatically pressed at 300 MPa to a green density of around 63 %. Density development, phase identification, shrinkage behavior and the microstructure were investigated to determine the sinterability of the developed glasses. The glass powders were sintered at different temperatures inside the processing window while crystallization was monitored. The results have shown that the sinterability of the developed glasses strongly depends on the proposed chemical additions. The highest density reached was 96 %, which belongs to BP1 glass with sintering conditions of 20 K/min heating rate for 60 min at 750 °C.

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Keywords

Bioactive glass, viscous sintering, crystallization, processing window, grain boundary

References

1 Jones, J.R., Lin, S., Yue, S., Lee, P.D., Hanna, J.V., Smith, M.E., et al.: Bioactive glass scaffolds for bone regeneration and their hierarchical characterization, Proc. Mech. Eng. Part H: J. Eng. Med., 224, 1373 – 1387, (2010).

2 Rahaman, M.N., Day, D.E., Bal, B.S., Fu, Q., Jung, S.B., Bonewald, L.F., et al.: Bioactive glass in tissue engineering, Acta Biomater., 7, 2355 – 2373, (2011).

3 Elgayar, I., Aliev, A.E., Boccaccini, A.R., Hill R.G.: Structural analysis of bioactive glasses, J. Non-Cryst. Solids, 315, 173 – 183, (2005).

4 Groh, D., Döhler, F., Brauer, D.S.: Bioactive glasses with improved processing. part 1. thermal properties, ion release and apatite formation, Acta Biomater., 10, 4465 – 4473, (2014).

5 Hmood, F., Goerke, O., Schmidt, F.: Chemical composition refining of bioactive glass for better processing features, part I, Biomed. Glasses, 4, 82 – 94, (2018).

6 Wu, Z.Y., Hill, R.G., Jones, J.R.: Optimizing the processing of porous melt-derived bioactive glass scaffolds, Bioceram. Dev. Appl., 1, 1 – 4, (2011).

7 Hmood, F., Guenster, J., Heinrich, J.G.: Sintering and piezoelectric properties of K0.5Na0.5NbO3 glass microspheres, J. Eur. Ceram. Soc., 35, 4143 – 4151, (2015).

8 Wadsworth, F.B., Vasseur, J., Llewellin, E.W., Schauroth, J., Dobson, K.J., Scheu, B., et al.: Sintering of viscous droplets under surface tension, Proc. R. Soc., A472, 20150780, (2016).

9 Cutler, I.B.: Sintering of glass powders during constant rates of heating, J. Am. Ceram. Soc., 52, 14 – 17, (1969).

10 Agea-Blanco, B., Reinsch, S., Müller, R.: Sintering and foaming of barium silicate glass powder compacts, Front. Mater., 3, 45, (2016).

11 Zanotto, E.D.: Glass crystallization research — A 36-year retrospective. part I, fundamental studies, Int. J. App. Glass Sci., 4, 105 – 116, (2013).

12 Boccaccini, A.R., Stumpfe, W., Taplin, D.M.R., Ponton, C.B.: Densification and crystallization of glass powder compacts during constant heating rate sintering, Mater. Sci. Eng., A219, 26 – 31, (1996).

13 Lefebvre, L., Gremillard, L., Chevalier, J., Zentai, R., Bernache-Assolant, D.: Sintering behavior of 45S5 Bioglass®, Key Eng. Mat., 361, 265 – 268, (2008).

14 Cormack, A.N., Tilocca, A.: Structure and bioactivity of glasses and ceramics, Philos. T. R. Soc. A, 370, 1271 – 1280, (2012).

15 Ciraldo, F.E., Boccardi, E., Melli, V., Westhauser, F., Boccaccini, A.R., Tackling bioactive glass excessive in vitro bioreactivity: Preconditioning approaches for cell culture tests, Acta Biomater., 75, 3 – 10, (2018).

16 Gerhardt, L., Boccaccini, A.R.: Bioactive glass and glass-ceramic scaffolds for bone tissue engineering, Materials, 3, 3867 – 3910, (2010).

17 Li, Z., Thompson, B.C., Hu, H., Kohr, K.: Rapid fabrication of dense 45S5 Bioglass® compacts through spark plasma sintering and evaluation of their in vitro biological properties, Biomed. Mater., 11, 065006, (2016).

18 Bretcanu, O., Chatzistavrou, X., Paraskevopoulos, K., Conradt, R., Thompson, I., Boccaccini, A.R.: Sintering and crystallization of 45S5 Bioglass® powder, J. Eur. Ceram. Soc., 29, 3299 – 3306, (2009).

19 Abe, K., Hamada, J., Miyazawa, M., Kuwahara, H., Itatani, K.: Fabrication of transparent sintered ZnO-B2O3-Bi2O3 glass body by pressureless firing and hot isostatic pressing, IOP Conf. Ser.: Mater. Sci. Eng., 47, 012024, (2013).

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