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Journal of Ceramic Science and Technology

The Journal of Ceramic Science and Technology publishes original scientific articles on all topics of ceramic science and technology from all ceramic branches. The focus is on the scientific exploration of  the relationships between processing, microstructure and properties of sintered ceramic materials as well as on new processing routes for innovative ceramic materials. The papers may have either theoretical or experimental background. A high quality of publications will be guaranteed by a thorough double blind peer review process.

The Journal is published by Göller Verlag GmbH on behalf of the Deutsche Keramische Gesellschaft (DKG). Edited by Yu-Ping Zeng, Shanghai Institute of Ceramics, Chinese Academy of Sciences, China.

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Er, Cr:YSGG and Nd:YAG Laser Surface Treatment of Lithium Disilicate Ceramics: SEM, EDX Analysis and Composite Bond Strength Evaluation

D.H.M. El Azzouni

Oral and Maxillofacial Prosthetic Department, College of Dentistry, King Abdulaziz University, Jeddah, KSA.

received October 30, 2025, received in revised form November 27, 2025, accepted November 27, 2025

Pages 1-8   DOI: 10.4416/JCST2025-00035

Abstract

This study is an evaluation of the impact of pre-treatment regimes –  Hydrofluoric Acid (HFA), Neodymium-doped Yttrium-Aluminum Garnet (Nd:YAG), and Erbium, Chromium: Yttrium-Scandium-Gallium-Garnet (Er,Cr:YSGG) laser – on the surface roughness (Ra), topography, and repair bond strength (RBS) of lithium disilicate ceramics (LDC) with micro-hybrid composite (MHC), having high-viscosity, and an injectable composite (IC) with low-viscosity. Ninety LDC disks were fabricated. The discs were divided into three groups according to surface pretreatment (n = 30 each). Group 1: HFA, Group 2: ErCr:YSGG, Group 3: Nd:YAG laser. To assess the Ra, five samples from each cohort were examined under a profilometer. Five samples from each surface treatment group were subjected to topographical evaluation by means of SEM. Twenty samples from each group were allocated into two groups determined by the viscosity of the resin composite. Low-viscosity IC(A) and high-viscosity MHC(B). A universal testing machine and a stereomicroscope were used to assess the RBS and failure modes. Statistical analysis was performed using ANOVA followed by post hoc Tukey, (p < 0.05). HFA-pretreated samples achieved the maximum Ra scores. Nd:YAG laser-treated LDC discs exhibited the minimum Ra scores. The highest bond strength was observed in Group 1A samples. Nd:YAG laser + MHC discs demonstrated the lowest RBS. HFA, as a surface conditioning regime, and a low-viscosity IC, as a repair material, displayed better performance in terms of improving surface characteristics and bond strength with LDC.

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Keywords

Hydrofluoric acid, micro-hybrid composite, injectable composite, lithium disilicate ceramics, surface topography

References

1 David, J., De Matos, M., Rocha, G., Lopes, S., Antonio Queiroz, D., Jiro, L., Nakano, N., Carvalho, N., Ribeiro, R., Barbosa, A.B., Anami, L.C., Bottino, M.A.: Dental ceramics: fabrication methods and aesthetic characterization, Coatings, 12, [8], 1228 – 1234, (2022).

2 Alkhudhairy, F., Naseem, M., Ahmad, Z.H., Alnooh, A.N., Vohra, F.: Efficacy of phototherapy with different conventional surface treatments on adhesive quality of lithium disilicate ceramics, Photodiagnosis Photodyn. Ther., 25, 292 – 295, (2019).

3 Makhija, S.K., Lawson, N.C., Gilbert, G.H., Litaker, M.S., McClelland, J.A., Louis, D.R., Gordan, V.V., Pihlstrom, D.J., Meyerowitz, C., Mungia, R., McCracken, M.S.: Dentist material selection for single-unit crowns: findings from the national dental practice-based research network, J. Dent., 55, 40 – 47, (2016).

4 Özdemir, H., Aladağ, L.İ.: Effect of different surface treatments on bond strength of different resin cements to lithium disilicate glass ceramic: an in vitro study, Biotechnol. Biotechnol. Equip., 31, [4], 815 – 820, (2017).

5 Yilmaz-Savas, T., Demir, N., Ozturk, A.N., Kilic, H.S.: Effect of different surface treatments on the bond strength of lithium disilicate ceramic to the zirconia core, Photomed. Laser Surg., 34, [6], 236 – 243, (2016).

6 Hofsteenge, J.W., Carvalho, M.A., Borghans, P.M., Cune, M.S., Özcan, M., Magne, P., Gresnigt, M.M.M.: Effect of preparation design on fracture strength of compromised molars restored with lithium disilicate inlay and overlay restorations: an in vitro and in silico study, J. Mech. Behav. Biomed. Mater., 146, (2023).

7 Alqarawi, F.K., Alhumaidan, A.A., Aldakhili, A., Alfayez, A., Abushowmi, T., Alramadan, A., Alzoubi, F.: Intraoral repair of fractured ceramics: A literature review, F1000Research, 11, 1275 – 1281, (2022).

8 Hickel, R., Mesinger, S., Opdam, N., Loomans, B., Frankenberger, R., Cadenaro, M., Burgess, J., Peschke, A., Heintze, S.D., Kühnisch, J.: Revised FDI criteria for evaluating direct and indirect dental restorations —recommendations for its clinical use, interpretation, and reporting, Clin. Oral Investig., 27, [6], 2593 – 2599, (2023).

9 Prado, M., Prochnow, C., Marchionatti, A.M.E., Baldissara, P., Valandro, L.F., Wandscher, V.F.: Ceramic surface treatment with a single-component primer: resin adhesion to glass ceramics, J. Adhes. Dent., 20, [2], 99 – 105, (2018).

10 Lanza, M.D.S., Rodrigues Lanza, F.J.S., Manso, A.P., Matinlinna, J.P., Carvalho, R.M.: Innovative surface treatments for improved ceramic bonding: lithium disilicate glass ceramic, Int. J. Adhes. Adhes., 82, 60 – 66, (2018).

11 Alkhudhairy, F., AlFawaz, Y.F.: Pretreatment of hybrid ceramics using Ho: YAG, low-level laser therapy activated malachite green, and non-thermal plasma on surface roughness, bond strength, and color change, SEM and EDX analysis, Ceramics, 7, [3], 944 – 957, (2024).

12 Alanazi, A.M., Khan, N.A., Khan, A.A., Ansari, Z., Shabbir, T., Leemani, M.J.: Lithium disilicate ceramics surface pre-treatment using low-level laser therapy-activated riboflavin, and Ti: Al2O3 laser on the colour change, surface roughness, and shear bond strength to adhesive cement: an in vitro SEM valuation, Ceram. - Silikaty, 69, [1], 93 – 100, (2025).

13 Kim, K.J., Park, Y.T., Yoo, J.H., Park, T.H.: Hydrofluoric acid burns, Exog. Dermatology, 3, [1], 12 – 18, (2004).

14 Vohra, F., Labban, N., Al-Hussaini, A., Al-Jarboua, M., Zawawi, R., Alrahlah, A., Naseem, M.: Influence of Er;Cr:YSGG laser on shear bond strength and color stability of lithium disilicate ceramics: an in vitro study, Photobiomodulation, Photomed., Laser Surg., 37, [8], 483 – 488, (2019).

15 Alkhudhairy, F., AlKheraif, A., Bin-Shuwaish, M., Al-Johany, S., Naseem, M., Vohra, F.: Effect of Er,Cr:YSGG laser and ascorbic acid on the bond strength and microleakage of bleached enamel surface, Photomed. Laser Surg., 36, [8], 1 – 8, (2018).

16 Maawadh, A.M., Almohareb, T., Al-Hamdan, R.S., Al Deeb, M., Naseem, M., Alhenaki, A.M., Vohra, F., Abduljabbar, T.: Repair strength and surface topography of lithium disilicate and hybrid resin ceramics with LLLT and photodynamic therapy in comparison to hydrofluoric acid, J. Appl. Biomater. Funct. Mater., 18, (2020).

17 Chen, L., Suh, B.: Bonding of resin materials to all-ceramics: a review, Curr. Res. Dent., 3, [1], 7 – 17, (2012).

18 da Silva, S.E.G., de Araújo, G.M., Souza, K.B., Moura, D.M.D., Aurélio, I.L., May, L.G., Vila-Nova, T.E.L., Zhang, Y., de Assunção e Souza, R.O.: Biaxial flexure strength and physicochemical characterization of a CAD/CAM lithium disilicate ceramic: effect of etching time, silane, and adhesive applications, Clin. Oral Investig., 26, [11], 6753 – 6763, (2022).

19 Alshahrani, A.: Post surface conditioning via air abrasion, Nd: YAG laser and radachlorin activated photodynamic therapy on surface roughness, surface topography, and bond strength to root dentin, Photodiagnosis Photodyn. Ther., 54, (2025).

20 Gorler, O., Dogan, D.O., Ulgey, M., Goze, A., Hubbezoğlu, I., Zan, R., Ozdemir, A.K.: The effects of Er:YAG, Nd:YAG, and Ho:YAG laser surface treatments to acrylic resin denture bases on the tensile bond strength of silicone-based resilient liners, Photomed. Laser Surg., 33, [8], 409 – 414, (2015).

21 Pirnat, S., Lukac, M., Ihan, A.: Study of the direct bactericidal effect of Nd:YAG and diode laser parameters used in endodontics on pigmented and nonpigmented bacteria, Lasers Med. Sci., 26, [6], 755 – 761, (2011).

22 Franke, M., Taylor, A.W., Lago, A., Fredel, M.C.: Influence of Nd:YAG laser irradiation on an adhesive restorative procedure, Oper. Dent., 31, [5], 604 – 609, (2006).

23 Liu, L., Liu, S., Song, X., Zhu, Q., Zhang, W.: Effect of Nd: YAG laser irradiation on surface properties and bond strength of zirconia ceramics, Lasers Med. Sci., 30, [2], 627 – 634, (2015).

24 Abu Hasna, A., Semmelmann, S., Feitosa, F.A., De Souza Andrade, D., Tay, F.R., Pucci, C.R.: Effect of Nd:YAG laser with/without graphite coating on bonding of lithium disilicate glass-ceramic to human dentin, Int. J. Dent., 2021, 6677159, (2021).

25 Rab, A., Siraj, K., Naz, S., Asghar, H., Irshad, M., Latif, A.: The influence of Nd: YAG pulsed laser treatment on the structure, morphology and hardness of e.max ceram dental material, Dig. J. Nanomater. Biostructures, 16, [4], 1519 – 1525, (2021).

26 Ozge, C., Yilmaz, N.A., Balin, E.: Effect of Er:Yag laser on repair bond strength of a nano hybrid composite, J. Stomatol., 75, [2], 122 – 129, (2022).

27 Shono, N.N., Alkhudhairy, F.: Repair bond strength in hybrid ceramic preconditioned with Ho: YAG laser and toluidine blue, activated by low-level laser therapy, using composites with varying viscosities: an analysis of surface topography and elemental analysis, Microsc. Res. Tech., 88, [10], 2754 – 2762, (2025).

28 Dapieve, K.S., Velho, H.C., da Rosa, L.S., Pivetta, J.P., Maidana, F.C., Venturini, A.B., Kleverlaan, C.J., Pereira, G.K.R., Valandro, L.F.: Ceramic surface conditioning, resin cement viscosity, and aging relationships affect the load-bearing capacity under fatigue of bonded glass-ceramics, J. Mech. Behav. Biomed. Mater., 139, (2023).

29 Aali, K.A.A.: Repair strength and roughness of resin matrix ceramic pretreated with rose bengal activated low level laser therapy and Er, Cr: YSGG bonded to different viscosity composites, Photodiagnosis Photodyn. Ther., 55, 104740 – 104747, (2025).

30 Aljamhan, A., Alkhudhairy, F.: Impact of hydrofluoric acid, ytterbium fiber lasers, and hydroxyapatite nanoparticles on surface roughness and bonding strength of resin cement with different viscosities to lithium disilicate glass ceramic: SEM and EDX analysis, Crystals, 15, [7], 661, (2025).

31 Alqahtani, S.A., Alsaeed, A.Y., Alqahtani, S.M., Shafqat, S., Niaz, M.O., Ishtiaque, Y., Abrar, E.: Lithium disilicate ceramics pretreated with Ti: sapphire fs, Er; Cr: YSGG, and Er: YAG lasers: a study on mechanical properties, energy dispersive spectroscopy, color alterations, and surface topography, Microsc. Res. Tech., 88, [11], 3029 – 3036, (2025).

32 Vohra, F., Labban, N., Al-Hussaini, A., Al-Jarboua, M., Zawawi, R., Alrahlah, A., Naseem, M.: Influence of Er;Cr:YSGG laser on shear bond strength and color stability of lithium disilicate ceramics: an in vitro study, Photobiomodulation, Photomed., Laser Surg., 37, [8], 483 – 488, (2019).

33 Albakri, A.S.: Pretreatment of hybrid ceramics using alumina (Al2O3) nanoparticles, hydrofluoric acid, and Holmium: YAG laser for optimizing surface roughness, shear bond strength, and topography, J. Biomater. Tissue Eng., 13, [12], 1133 – 1138, (2024).

34 Almohareb, T., Maawadh, A., AlDeeb, L., Alahdal, K., Alshamrani, A.S., Alrahlah, A.: Influence of high- and low-viscosity resin cement and artificial aging on bond integrity and surface roughness of lithium disilicate ceramics pretreated with Ho:YAG laser and nano-hydroxyapatite coatings, J. Ceram. Sci. Tech., 16, [1], 29 – 36, (2025).

35 Kern, M., Barloi, A., Yang, B.: Surface conditioning influences zirconia ceramic bonding, J. Dent. Res., 88, [9], 817 – 822, (2009).

36 Lyann, S.K., Takagaki, T., Nikaido, T., Uo, M., Ikeda, M., Sadr, A., Tagami, J.: Effect of different surface treatments on the tensile bond strength to lithium disilicate glass ceramics, J. Adhes. Dent., 20, [3], 483 – 488, (2018).

37 Alrabeah, G., Alhamid, R.F., Alamer, B.A., Alrajhi, F.N., Binrayes, A., Habib, S.R.: Impact of various surface treatments on the shear bond strength between lithium disilicate ceramics and resin cement, Front. Mater., 11, 54 – 62 (2024).

38 Levartovsky, S., Bohbot, H., Shem-Tov, K., Brosh, T., Pilo, R.: Effect of different surface treatments of lithium disilicate on the adhesive properties of resin cements, Materials, 14, [12], 3302, (2021).

39 Al-Askary, R.A., Al-Ashou, W.M.O., Hassoon, S.N.: Repair bond strength of composite resin to dental ceramic using various surface treatments: an in vitro study, J. Int. Soc. Prev. Community Dent., 14, [5], 388 – 395, (2024).

40 Degirmenci, A., Unalan Degirmenci, B.: Effects of Er,Cr:YSGG laser surface treatments and composites with different viscosities on the repair bond strength of CAD/CAM resin nanoceramic, Polymers, 16, [15], 2212, (2024).

41 Al-Karadaghi, S.S., Jawad, H., Al-Karadaghi, T.: The influence of pulse duration and exposure time of Er,Cr:YSGG laser on lithium disilicate laminate debonding, an in vitro study, Heliyon, 9, [3], e14600, (2023).

42 Chegeni, E., Espanã-Tost, A., Figueiredo, R., Valmaseda-Castellón, E., Arnabat-Domínguez, J.: Effect of an Er,Cr:YSGG laser on the surface of implants: a descriptive comparative study of 3 different tips and pulse energies, Dent. J., 8, [4], 109, (2020).

43 Ataol, A.S., Ergun, G.: Repair bond strength of resin composite to bilayer dental ceramics, J. Adv. Prosthodont., 10, [2], 101 – 112, (2018).

44 Ebrahimi Chaharom, M.E., Pournaghi Azar, F., Mohammadi, N., Nasiri, R.: Effect of surface preparation with Nd:YAG and Er,Cr:YSGG lasers on the repair bond strength of lithium disilicate glass ceramic to a silorane-based composite resin, J. Dent. Res. Dent. Clin. Dent. Prospects, 12, [1], 12 – 17, (2018).

45 Akyil, M.Ş., Yilmaz, A., Karaalioğlu, O.F., Duymuş, Z.Y.: Shear bond strength of repair composite resin to an acid-etched and a laser-irradiated feldspathic ceramic surface, Photomed. Laser Surg., 28, [4], 539 – 545, (2010).

46 Alizadeh Oskoee, P., Mohammadi, N., Ebrahimi Chaharom, M.E., Kimyai, S., Pournaghi Azar, F., Rikhtegaran, S., Shojaeei, M.: Effect of surface treatment with Er;Cr:YSSG, Nd:YAG, and CO2 lasers on repair shear bond strength of a silorane-based composite resin, J. Dent. Res. Dent. Clin. Dent. Prospects, 7, [2], 61 – 66, (2013).

47 Ozge, C., Yilmaz, N.A., Balin, E.: Effect of Er: YAG laser on repair bond strength of a nano hybrid composite, J. Stomatol., 75, [2], 122 – 129, (2022).

48 Abu Hasna, A., Semmelmann, S., Feitosa, F.A., De Souza Andrade, D., Tay, F.R., Pucci, C.R.: Effect of Nd:YAG laser with/without graphite coating on bonding of lithium disilicate glass-ceramic to human dentin, Int. J. Dent., 2021, 391 – 398, (2021).

49 Degirmenci, A., Unalan Degirmenci, B.: Effects of Er,Cr:YSGG laser surface treatments and composites with different viscosities on the repair bond strength of CAD/CAM resin nanoceramic, Polymers, 16, [15], 2212, (2024).

50 Kemaloglu, H., Cay, O., Ercan Devrimci, E., Pamir, T.: Repair bond strength of a new self-adhesive composite resin to three different resin-matrix ceramic CAD-CAM materials, Dent. Mater. J., 43, [2], 137 – 145, (2024).

51 Sismanoglu, S., Yildirim-Bilmez, Z., Erten-Taysi, A., Ercal, P.: Influence of different surface treatments and universal adhesives on the repair of CAD-CAM composite resins: an in vitro study, J. Prosthet. Dent., 124, [2], 238.e1 – 238.e9, (2020).

52 Lopes, G.C., Perdigão, J., Baptista, D., Ballarin, A.: Does a self-etching ceramic primer improve bonding to lithium disilicate ceramics? bond strengths and FeSEM analyses, Oper. Dent., 44, [2], 210 – 218, (2019).

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