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Effect of Pre-Treatment Techniques Nd: YLF laser, Nano-HAp Particles on Surface Roughness and Repair Bond Strength of Different-Viscosity Composite Bonded to Hybrid Ceramics
Abdullah Aljamhan, Fahad Alkhudhairy
Restorative Dental Sciences Department, College of Dentistry, King Saud University, Riyadh, Saudi Arabia.
received May 12, 2025, received in revised form June 5, 2025, accepted June 18, 2025
Vol. 16, No. 4, Pages 263-268 DOI: 10.4416/JCST2025-00014
Abstract
Evaluating the effect of airborne particle abrasion (APA), Nd: YLF laser, hydroxyapatite nanoparticles (Nano-HAp) on surface roughness (Ra), topography, and repair bond strength (RBS) of different-viscosity composites bonded to hybrid ceramic (HBC). 78 CAD/CAM HBC discs were prepared and divided into three groups based on surface treatment (n = 26). Group 1: APA, Group 2: Nd: YLF laser, and Group 3: Nano-HAp coating. A surface profilometer measured the Ra scores (n = 5 each). SEM was used for surface topography (n = 1 each). On the remaining samples, an adhesive was applied and cured. Twenty samples from each group were further categorized into two subgroups based on the composite viscosity. Bond strength and failure mode were assessed. A one-way ANOVA and a Tukey test were conducted to identify significant differences among groups. The highest mean Ra score was exhibited by Group 2 (Nano-HAp). Group 3 (Nd:YLF laser)-conditioned samples demonstrated the lowest Ra. Maximum RBS values were observed for Group 2B (Nano-HAp+Injectable). The minimum bond strength was noted for Nd: YLF laser+Microhybrid. Lower-viscosity composite displayed better performance than conventional composite. The most successful method for surface preparation of HBC involves pretreating with Nano-HAp coating. The use of a low-viscosity injectable composite as the repair material results in enhanced bond strength.
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Keywords
Hydroxyapatite, hybrid ceramic, roughness, bond strength, scanning electron microscopy
References
1 Shabib, S.: Use of Nd:YVO4 laser, photodynamic therapy, sulfuric acid and sand blasting on improving bond integrity of PEEK to resin cement with adhesive, Photodiagnosis Photodyn Ther., 39, 102865 – 102871, (2022).
2 David, J., De Matos, M., Rocha, G. et al.: Dental Ceramics: fabrication methods and aesthetic characterization, Coatings, 12, [8], 1228 – 1234, (2022).
3 Topbaş, C., Çınar, Ş., Altan, B.: The effects of different root canal irrigation protocols and artificial aging procedures on the bond strength between dentin and hybrid ceramic posts, BMC Oral Health; 22, [1], 5879 – 5885, (2022).
4 Samolyuk, G.D., Edmondson, P.D.: First principles study of the stability and thermal conductivity of novel li-be hybrid ceramics, Acta Mater., 215, [3], 117052 – 117059, (2021).
5 Aurélio, I.L., Fraga, S., Dorneles, L.S. et al.: Extended glaze firing improves flexural strength of a glass ceramic, Dent. Mater., 31, [12], e316 – e324, (2015).
6 Maawadh, A.M., Almohareb, T., Al-Hamdan, R.S.: Repair strength and surface topography of lithium disilicate and hybrid resin ceramics with LLLT and photodynamic therapy in comparison to hydrofluoric acid, J. Appl. Biomater. Funct. Mater., 18, (2020).
7 Uhrenbacher, J., Schmidlin, P.R., Keul, C.: The effect of surface modification on the retention strength of polyetheretherketone crowns adhesively bonded to dentin abutments, J. Prosthet. Dent., 112, [6], 1489 – 1497, (2014).
8 Shimoe, S., Peng, T.Y., Otaku, M.: Influence of various airborne-particle abrasion conditions on bonding between zirconia ceramics and an indirect composite resin material, J. Prosthet. Dent., 122, [5], 491.e1 – 491.e9, (2019).
9 Alkhudhairy, F., Naseem, M., Ahmad, Z.H.: Efficacy of phototherapy with different conventional surface treatments on adhesive quality of lithium disilicate ceramics, Photodiagnosis Photodyn. Ther., 25, [3], 292 – 295, (2019).
10 Alrahlah, A., Naseem, M., Tanveer, S.A.: Influence of disinfection of caries effected dentin with different concentration of silver diamine fluoride, curcumin and er, Cr:YSGG on adhesive bond strength to resin composite, Photodiagnosis Photodyn. Ther., 32, [2], 1478 – 1485, (2022).
11 Al-Qahtani, A.S., AlZain, S.A., AlHamdan, E.M.: A comparative evaluation of the effect of phototherapy of fiber post on its bond strength to dental composite, Photodiagnosis Photodyn. Ther., 24, [3] 228 – 231, (2018).
12 Niemz, M.H.: Cavity preparation with the Nd:YLF picosecond laser, J. Dent. Res., 74, [5], 1194 – 1199, (1995).
13 Almohareb, T., Maawadh, A., AlDeeb, L.: Influence of High- and low-viscosity resin cement and artificial aging on bond integrity and surface roughness of lithium disilicate ceramics pretreated with Ho:YAG laser and nano-hydroxyapatite coatings, J. Ceram. Sci. Technol., 16, [1], 29 – 36, (2025).
14 Bordina, G.E., Lopina, N.P., Andreev, A.A.: Comparative characteristics of the chemical structure of ormokers and traditional composites, Russ. J. Dent. 26, [6], 503 – 512, (2022).
15 Cidreira Boaro, L.C., Pereira Lopes, D., de Souza, A.S.C. et al.: Clinical performance and chemical-physical properties of bulk fill composites resin – a systematic review and meta-analysis, Dent. Mater., 35, [10], e249 – e264, (2019).
16 Zanatta, C.T.I., de Favori Cardoso, P.M., Camilotti, V.: Micro-shear bond strength of self-adhesive versus conventional low-viscosity composite Resins: in vitro study, J. Adv. Med. Med. Res., 36, [4], 11 – 20, (2024).
17 Chuenjit, P., Suzuki, M., Shinkai, K.: Effect of various surface treatments on the bond strength of resin luting agent and the surface roughness and surface energy of CAD/CAM materials, Dent. Mater. J., 40, [1], 16 – 25, (2021).
18 Niizuma, Y., Kobayashi, M., Toyama, T.: Effect of etching with low concentration hydrofluoric acid on the bond strength of CAD/CAM resin block, Dent. Mater. J., 39, [6], 1000 – 1008, (2020).
19 Awada, A., Nathanson, D.: Mechanical Properties of Resin-Ceramic CAD/CAM Restorative Materials Presented at the American Association of Dental Research/Canadian Association of Dental Research Annual Meeting, Charlotte, NC, March 2014. J. Prosthet. Dent., 114, [4], 587 – 593, (2015).
20 García-Sanz, V., Paredes-Gallardo, V., Bellot-Arcís, C. et al.: Effects of femtosecond laser and other surface treatments on the bond strength of metallic and ceramic orthodontic brackets to zirconia, PLoS One, 12, [10], 874 – 882, (2017).
21 Asik, B., Ozyilmaz, O.Y.: Effects of various laser applications on surface roughness and bond strength to veneering composites of polyether ether ketone (PEEK) and polyether ketone ketone (PEKK) materials, Lasers Med. Sci., 39, [1], 269 – 275, (2024).
22 Dapieve, K.S., Pereira, G.K.R., Venturini, A.B.: Do Resin Cement Viscosity and Ceramic Surface Etching Influence the Fatigue Performance of Bonded Lithium Disilicate Glass-Ceramic Crowns? Dent. Mater., 38, [3], e59 – e67, (2022).
23 Ozturk Yesilirmak, S., Oglakci, B., Ozduman, Z.C.: Shear bond strength of repaired CAD/CAM resin-based composite materials submitted to Er:YAG laser treatments at different powers, Coatings, 13, [9], 1 – 9, (2023).
24 Gale, M.S., Darvell, B.W.: Thermal cycling procedures for laboratory testing of dental restorations, J. Dent., 27, [2], 89 – 99, (1999).
25 Aladağ, S.Ü., Ayaz, E.A.: Repair bond strength of different CAD-CAM ceramics after various surface treatments combined with laser irradiation, Lasers Med. Sci., 38, [1], 478 – 484, (2023).
26 Kemaloglu, H., Cay, O., Ercan Devrimci, E.: Repair bond strength of a new self-adhesive composite resin to three different resin-matrix ceramic CAD-CAM materials, Dent. Mater. J., 43, [2], 137 – 145, (2024).
27 Ong, J.L., Chan, D.C.N.: Hydroxyapatite and their use as coatings in dental Implants: A review, Crit. Rev. Biomed. Eng., 28, [5 – 6], 667 – 707, (2000).
28 Lee, S.W., Hahn, B.D., Kang, T.Y.: Hydroxyapatite and collagen combination-coated dental implants display better bone formation in the peri-implant area than the same combination plus bone morphogenetic Protein-2-coated implants, hydroxyapatite-coated implants, and uncoated implants, J. Oral Maxillofac. Surg., 72, [1], 53 – 60, (2014).
29 Maawadh, A.M., Almohareb, T., Al-Hamdan, R.S.: Repair strength and surface topography of lithium disilicate and hy brid resin ceramics with LLLT and photodynamic therapy in comparison to hydrofluoric acid, J. Appl. Biomater. Funct. Mater., 18, (2020).
30 Jung, U.W., Hwang, J.W., Choi, D.Y.: Surface characteristics of a novel hydroxyapatite-coated dental implant, J. Periodontal Implant Sci., 42, [2], 59 – 63, (2012).
31 Alsunbul, H., Almutairi, B., Aljanakh, M.: Hybrid ceramic repair strength, surface roughness, and bond failure, using methylene blue-activated low-level laser therapy, carbon dioxide, and Ti: Al2O3 laser, Photodiagnosis Photodyn. Ther., 43, (2023).
32 Kim, J.E., Lim, J.H., Kang, Y.J.: Effect of pressure and particle size during aluminum oxide air abrasion on the flexural strength of disperse-filled composite and polymer-infiltrated ceramic network materials, Polymers, 12, [6], 745 – 755, (2020).
33 Barbon, F.J., Moraes, R.R., Isolan, C.P.: Influence of inorganic filler content of resin luting agents and use of adhesive on the performance of bonded ceramic, J. Prosthet. Dent., 122, [6], 566 e1 – 566.e11, (2019).
34 Moura, D.M.D., de Araújo, A.M.M,, de Souza, K.B.: Hydrofluoric acid concentration, time and use of phosphoric acid on the bond strength of feldspathic ceramics, Braz. Oral Res., 34, [3], 458 – 465, (2021).
35 Kilinc, H., Sanal, F.A, Turgut, S.: Shear bond strengths of aged and non-aged CAD/CAM materials after different surface treatments, J. Adv. Prosthodont., 12, [5], 273 – 282, (2020)
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